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informatica:hp_z400_600_topspin363_1 [2021/08/19 12:24] miquel created |
informatica:hp_z400_600_topspin363_1 [2021/08/19 16:09] (current) miquel [Configuració de l'espectròmetre] |
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====== Avance III 600 MHz - Instal·lació del Topspin 3.6.3 ====== | ====== Avance III 600 MHz - Instal·lació del Topspin 3.6.3 ====== | ||
+ | |||
+ | ===== Instal·lació del Topspin 3.6.3 ===== | ||
Instal·lo el TopSpin 3.6.3 a partir del fitxer d' | Instal·lo el TopSpin 3.6.3 a partir del fitxer d' | ||
Line 41: | Line 43: | ||
* NMR-Data: ''/ | * NMR-Data: ''/ | ||
- | <WRAP alert> | + | Defineixo '' |
- | Caldrà comprovar aquests instruccions | + | |
- | </WRAP> | + | A continuació comença el procés d' |
+ | |||
+ | * extracció dels fitxers de distribució comprimits, | ||
+ | * còpia de les carpetes i fitxers a la carpeta del TopSpin, etc. | ||
+ | |||
+ | Es nota que el disc dur és d' | ||
+ | |||
+ | Per acabar premo el botó <key>Finish</ | ||
+ | |||
+ | ===== Posada en funcionament del TopSpin 3.6.3 ===== | ||
+ | |||
+ | Poso en marxa el TopSpin per primer cop, i no detecta la consola, | ||
+ | |||
+ | < | ||
+ | TopSpin 3.6.3 | ||
+ | Installation directory: "/ | ||
+ | Waiting for CodeMeter license | ||
+ | |||
+ | 2021-08-11 12: | ||
+ | Cannot checkout TopSpin CodeMeter license | ||
+ | No matching license entry found for feature " | ||
+ | CmContainer Entry not found, Error 200. | ||
+ | |||
+ | CodeMeter Runtime Version: 7.10.4196 | ||
+ | empty CodeMeter Server Search List Configuration | ||
+ | |||
+ | If your workstation controls the spectrometer, | ||
+ | you may run the program without license. | ||
+ | This requires the acquisition server to be ready. | ||
+ | |||
+ | checking connection to spectrometer (may last several minutes) | ||
+ | no spectrometer service license available | ||
+ | </ | ||
+ | |||
+ | segurament perquè cal reiniciar-la perquè es descarregui el nou // | ||
+ | |||
+ | Premo el botó < | ||
+ | |||
+ | Per resoldre el problema amb la xarxa de l' | ||
+ | |||
+ | < | ||
+ | # cat hosts | ||
+ | ## 127.0.0.1 | ||
+ | ### ::1 localhost localhost.localdomain localhost6 localhost6.localdomain6 | ||
+ | |||
+ | 127.0.0.1 | ||
+ | 158.109.56.18 | ||
+ | |||
+ | # The following lines are related to Bruker NMR spectrometers | ||
+ | # DO NOT REMOVE THEM. | ||
+ | # | ||
+ | # An older TS version? | ||
+ | # 149.236.99.99 | ||
+ | |||
+ | # TS 3.6.3 | ||
+ | 149.236.99.90 | ||
+ | |||
+ | 149.236.99.1 | ||
+ | |||
+ | [...] | ||
+ | </ | ||
+ | |||
+ | i a Wireshark puc veure que ja s' | ||
+ | |||
+ | Comprovo l' | ||
+ | |||
+ | < | ||
+ | # systemctl status tftp | ||
+ | ● tftp.service - Tftp Server | ||
+ | | ||
+ | | ||
+ | Docs: man: | ||
+ | [root@cie-56-18 etc]# | ||
+ | [root@cie-56-18 etc]# | ||
+ | [root@cie-56-18 etc]# systemctl start tftp | ||
+ | [root@cie-56-18 etc]# systemctl status tftp | ||
+ | ● tftp.service - Tftp Server | ||
+ | | ||
+ | | ||
+ | Docs: man: | ||
+ | Main PID: 22927 (in.tftpd) | ||
+ | | ||
+ | | ||
+ | |||
+ | Aug 11 13:16:53 cie-56-18.uab.cat systemd[1]: Started Tftp Server. | ||
+ | </ | ||
+ | |||
+ | i només posar-lo en marxa, Wireshark mostra que l'IPSO s'ha pogut connectar i que està descarregant el seu sistema operatiu, i una estona després, ja hi ha connexió entre l' | ||
+ | |||
+ | < | ||
+ | # ping -c 5 149.236.99.90 | ||
+ | PING 149.236.99.90 (149.236.99.90) 56(84) bytes of data. | ||
+ | 64 bytes from 149.236.99.90: | ||
+ | 64 bytes from 149.236.99.90: | ||
+ | 64 bytes from 149.236.99.90: | ||
+ | 64 bytes from 149.236.99.90: | ||
+ | 64 bytes from 149.236.99.90: | ||
+ | |||
+ | --- 149.236.99.90 ping statistics --- | ||
+ | 5 packets transmitted, | ||
+ | rtt min/ | ||
+ | </ | ||
+ | |||
+ | Torno a posar en marxa el TopSpin i aquest cop detecta la consola i arrenca amb la " | ||
+ | |||
+ | < | ||
+ | TopSpin 3.6.3 - Copyright (C) 2021 Bruker BioSpin GmbH | ||
+ | Installation directory: "/ | ||
+ | Waiting for CodeMeter license | ||
+ | |||
+ | 2021-08-11 13: | ||
+ | Cannot checkout TopSpin CodeMeter license | ||
+ | No matching license entry found for feature " | ||
+ | CmContainer Entry not found, Error 200. | ||
+ | |||
+ | CodeMeter Runtime Version: 7.10.4196 | ||
+ | empty CodeMeter Server Search List Configuration | ||
+ | |||
+ | If your workstation controls the spectrometer, | ||
+ | you may run the program without license. | ||
+ | This requires the acquisition server to be ready. | ||
+ | |||
+ | checking connection to spectrometer (may last several minutes) | ||
+ | CPR : 2021-08-11 13: | ||
+ | TopSpin is currently running under | ||
+ | the spectrometer service license. | ||
+ | Please apply to receive a correct | ||
+ | license for your workstation | ||
+ | using the online license form: | ||
+ | https:// | ||
+ | </file> | ||
===== Configuració de l' | ===== Configuració de l' | ||
- | Al final de la instal·lació | + | Un cop es posa en marxa el TopSpin, |
Executo '' | Executo '' | ||
Line 81: | Line 213: | ||
malauradament per ara no el puc posar en marxa. | malauradament per ara no el puc posar en marxa. | ||
- | Després de reiniciar els amplificadors, | + | Després de reiniciar els amplificadors, |
+ | |||
+ | ==== Fitxer "uxnmr.info" ==== | ||
+ | |||
+ | < | ||
+ | # cat uxnmr.info | ||
+ | CONFIGURATION INFORMATION | ||
+ | ========================= | ||
+ | |||
+ | Path : / | ||
+ | Date : Fri Aug 13 09:38:41 2021 | ||
+ | Release | ||
+ | Installed in : / | ||
+ | Host : cie-56-18.uab.cat | ||
+ | OS : CentOS Linux release 7.9.2009 (Core) | ||
+ | CPU : Intel(R) Xeon(R) CPU W3550 @ 3.07GHz (4 cores at 3067 MHz) | ||
+ | User : sermnuab | ||
+ | System | ||
+ | 1H-frequency : 600.13 MHz | ||
+ | Description | ||
+ | Location | ||
+ | Bruker Order : PH000806 | ||
+ | Configured in: cie-56-18.uab.cat:/ | ||
+ | |||
+ | IPSO: connected to spectrometer subnet | ||
+ | - TCP/IP address = 149.236.99.90 | ||
+ | - IPSO type: 19" | ||
+ | - Tctrl : 1 | ||
+ | - Fctrls: 3 | ||
+ | - Gctrl1: with digital preemphasis | ||
+ | - Rctrl : none | ||
+ | - FREDs : none | ||
+ | - DPP : 1 | ||
+ | |||
+ | DRU1: DEB_DEFAULT | ||
+ | - TCP/IP address = 149.236.99.77 | ||
+ | - Firmware Version = 170619 | ||
+ | - DRU1 controls AQS-Rack and HPPR/2 | ||
+ | |||
+ | AQS: connected to 149.236.99.77:/ | ||
+ | _Slot_ SBSB _____________________Board_____________________ | ||
+ | Number Addr Type HW-VS FW-VS ID ECL Name | ||
+ | ----------------------------------------------------------- | ||
+ | | ||
+ | | ||
+ | | ||
+ | | ||
+ | | ||
+ | 21 0x21 0xcf | ||
+ | -- 0x20 0xc6 | ||
+ | | ||
+ | Logical Receiver/ | ||
+ | |||
+ | |||
+ | Router: none installed | ||
+ | |||
+ | Transmitters at the spectrometer subnet: | ||
+ | ---------------------------------------- | ||
+ | BLA_W1345096_0091 W1345096/ | ||
+ | - TCP/IP address = 149.236.99.93 | ||
+ | - Firmware VS = 20120627 | ||
+ | - Amplifier | ||
+ | - Router | ||
+ | - Controller | ||
+ | BLA_W1345092_0060 W1345092/ | ||
+ | - TCP/IP address = 149.236.99.92 | ||
+ | - Firmware VS = 20120627 | ||
+ | - Amplifier | ||
+ | - Router | ||
+ | - Controller | ||
+ | |||
+ | Gradient amplifiers at the spectrometer subnet: | ||
+ | ---------------------------------------------- | ||
+ | BGA1: BGA_W1213891_0009 | ||
+ | - TCP/IP address | ||
+ | - Firmware version = 20080206 | ||
+ | - Web version | ||
+ | - Current limits | ||
+ | |||
+ | BSMS: BSMS/2 connected to ethernet | ||
+ | - TCP/IP address = 149.236.99.20 | ||
+ | - ELCB firmware version = 20210212 | ||
+ | - SCB channels = 40 | ||
+ | - Shim System = BOSS2-SB | ||
+ | - 2HTX Amplifier: not available | ||
+ | - Lock: installed | ||
+ | - VTU_SPB = BSMS/2 SPB-E SENSOR & PNEUMATIC BD: Z115192/ | ||
+ | - VTU_VPSB1 = BSMS/2 VARIABLE POWER SUPPLY BD: Z115193/ | ||
+ | |||
+ | VTU: in BSMS/2 connected to ethernet | ||
+ | - TCP/IP address = 149.236.99.20 | ||
+ | |||
+ | SampleCase: in BSMS/2 connected to ethernet | ||
+ | - TCP/IP address = 149.236.99.20 | ||
+ | |||
+ | Bruker Automatic Changer: device connected to 149.236.99.90:/ | ||
+ | - Capacity: 24 holders | ||
+ | - Firmware: 970111 | ||
+ | - use BACS air = yes | ||
+ | - BACS sx delay = 10 s | ||
+ | - Sample Rail fast changer mode = no | ||
+ | |||
+ | Eurotherm VTU: device connected to 149.236.99.90:/ | ||
+ | - (used by TopSpin) | ||
+ | |||
+ | Preamplifiers : | ||
+ | HPPR2: - HPPR/2 preamplifier connected to 149.236.99.77:/ | ||
+ | Type : HPPR/2 | ||
+ | Controller: Cover/1 with Application firmware = AQ | ||
+ | 15 LEDs for tuning, 15 LEDs for matching | ||
+ | Module | ||
+ | PN=Z003462, SN=00485 from 20061101 | ||
+ | Module | ||
+ | PN=Z003506, SN=00529 from 20061024 | ||
+ | Module | ||
+ | PN=Z003473, SN=00491 from 20061206 | ||
+ | |||
+ | Gradient Controller cable connections | ||
+ | -------------------------------------------------------------------- | ||
+ | GCtrl1: connected via DPP to GREAT 1-10 Gradient Amplifier Unit W1213891/ | ||
+ | |||
+ | RF cable connections (detected) | ||
+ | -------------------------------------------------------------------- | ||
+ | SGU1 NORM output -> input 1 of transmitter 1 (BLAXH2H300/ | ||
+ | SGU1 AUX output -> input 4 of transmitter 1 (BLAXH2H300/ | ||
+ | SGU2 NORM output -> input 2 of transmitter 1 (BLAXH2H300/ | ||
+ | SGU2 AUX output -> TUNE signal input of HPPR | ||
+ | SGU3 NORM output -> input 3 of transmitter 1 (BLAXH2H300/ | ||
+ | SGU3 AUX output -> input 1 of transmitter 2 (BLAX300 E 6-365MHZ W1345092/ | ||
+ | |||
+ | Blanking cable connections (detected) | ||
+ | -------------------------------------------------------------------- | ||
+ | transmitter 1 = BLAXH2H300/ | ||
+ | - amplifier 1H-100W uses blanking 2 | ||
+ | - amplifier X-300W uses blanking 1 | ||
+ | - amplifier 2H-150W needs no blanking | ||
+ | |||
+ | transmitter 2 = BLAX300 E 6-365MHZ W1345092/ | ||
+ | - amplifier X-300W uses blanking 3 | ||
+ | </ | ||
+ | |||
+ | ==== Fitxers de configuració de les connexions RS232 ==== | ||
+ | |||
+ | La configuració de les connexions per port sèrie (RS232) també coincideix amb la del mes de maig, | ||
+ | |||
+ | < | ||
+ | # for FILE in ./ | ||
+ | > do | ||
+ | > echo $FILE | ||
+ | > cat $FILE | ||
+ | > echo | ||
+ | > done | ||
+ | |||
+ | ./ | ||
+ | # TOPSPIN alpha TTY configuration file | ||
+ | # created automatically by ' | ||
+ | # do not edit, changes are lost after next ' | ||
+ | unit = AQS | ||
+ | host = 149.236.99.77 | ||
+ | device = / | ||
+ | type = RS485 | ||
+ | stty = 9600 min 1 time 50 cs8 hupcl cread clocal | ||
+ | |||
+ | ./ | ||
+ | # TOPSPIN alpha TTY configuration file | ||
+ | # created automatically by ' | ||
+ | # do not edit, changes are lost after next ' | ||
+ | unit = Bruker Automatic Changer | ||
+ | host = 149.236.99.90 | ||
+ | device = / | ||
+ | type = RS232 | ||
+ | stty = 9600 min 1 time 50 cs8 hupcl cread clocal | ||
+ | |||
+ | ./ | ||
+ | # TOPSPIN alpha TTY configuration file | ||
+ | # created automatically by ' | ||
+ | # do not edit, changes are lost after next ' | ||
+ | unit = HPPR/2 preamplifier | ||
+ | host = 149.236.99.77 | ||
+ | device = / | ||
+ | type = RS485 | ||
+ | stty = 9600 min 1 time 50 cs8 hupcl cread clocal | ||
+ | |||
+ | ./ | ||
+ | # TOPSPIN alpha TTY configuration file | ||
+ | # created automatically by ' | ||
+ | # do not edit, changes are lost after next ' | ||
+ | unit = Eurotherm VTU | ||
+ | host = 149.236.99.90 | ||
+ | device = / | ||
+ | type = RS232 | ||
+ | stty = 9600 time 5 parenb cs7 cread clocal istrip | ||
+ | </ | ||
+ |