;Pulse Program Code for Bruker: ;pp:zprof ;1D Experiment ;1D z-profile image of the sample ;Evaluation of the excitation achieved in the z direction when multiple-frequency pulses are applied in spatially encoded NMR experiments. ;Avance III version ;Topspin 2.1 & Topspin 3.1 ;1D sequence ;Modified by Laura Castañar (12/03/2013) ;L. Castañar, P. Nolis, A. Virgili and T. Parella. Chem. Eur. J. 2013,19, 15472–1547. ;DOI: http://dx.doi.org/10.1002/chem.201303272 ;Original pp:echograd4 ;This pulse program has been created by Patrick Giraudeau and Serge Akoka, CEISAM, University of Nantes, France ;The authors are not responsible for the results obtained with this pulse sequence, and decline responsibility for any damage resulting from the use of this program ;Please refer to the protocol provided with this pulse sequence for correctly adjusting acquisition and processing parameters ;Please do not delete this header from the pulse program. #include #include "p2=p1*2" 1 ze 200u UNBLKGRAD 2 d1 4u pl0:f1 200u gron0 p12:sp2:f1 ph10 200u groff 1m pl1:f1 p1 ph1 d2 gron1 200u groff d3 p2 ph2 d4 d5 gron2 go=2 ph31 1m groff 100u BLKGRAD 30m mc #0 to 2 F0(zd) exit ph1=0 ph2=0 2 1 3 ph10=0 ph31=0 0 2 2 ;pl1: f1 channel - power level for pulse (default) ;p1: f1 channel - 90 degree high power pulse [us] ;p2: f1 channel - 180 degree high power pulse [us] ;p12: f1 channel - 180 degree high power selective pulse [ms] ;sp2: shaped pulse power level for selective excitation ;spnam2: shaped pulse for selective excitation ;d1: relaxation delay [1s] (only one scan is recorded) ;d2: duration of refocusing gradient [10ms] ;d3: delay adjusted for observation of echo [1ms] ;d4: delay adjusted for observation of echo [1ms] ;d5: acquisition gradient delay before opening receiver [5ms] ;de: 10u ;ds: 0 ;GPZ0: encoding gradient [0-100] ;GPZ1: defocusing gradient ;GPZ2: refocusing gradient GPZ2=GPZ1. ;NS: 1*n ;AQ_mod: DQD (AvanceIII) ;SW: maximum value allowed by the spectrometer