“Full sensitivity and enhanced resolution in homodecoupled band-selective NMR experiments” by Laura Castañar, Pau Nolis, Albert Virgili and Teodor Parella. Chem. Eur. J. 2013, 19, 17283-17286.
A NMR pulse scheme that provides full sensitivity in homodecouped band-selective NMR experiments is proposed. The easy implementation of this HOBS scheme as a general building block into a great variety of multidimensional NMR experiments leads to pure-shift spectra with enhanced resolution and with the maximum attainable sensitivity.
Pulse Programs Code for Bruker:
- 1D HOmodecoupling Band-Selective (HOBS)
- 2D HOBS-TOCSY
- 2D non-refocused F2-coupled HOBS-HSQC
- 2D refocused F2-coupled HOBS-HSQC-CLIP
- 2D refocused homo- and heteronuclear decoupled HOBS-HSQC
Data set Example:
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