Measuring heteronuclear long range connectivities.

The optimum detection and accurate measurement of longer-range ( 4 J and higher) heteronuclear NMR correlations is described. The magnitude and/or the sign of a wide range of large and small long-range couplings can be simultaneously determined for protonated and non-protonated 13 C and 15 N nuclei using the LR-selHSQMBC experiment.

 

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