Rapid and efficient enantiodifferentiation through frequency-selective pure-shift ¹H NMR spectroscopy

2014-03-06Methods & Applications, Our Publications, Our Researchband-selective, enantiodifferentiation, enhanced resolution, full sensitivity, HOBS, homodecoupling, homonuclear decoupling, pure-shift NMRLaura

“Enantiodifferentiation through Frequency-Selective Pure-Shift 1H Nuclear Magnetic Resonance Spectroscopy” by Laura Castañar, Míriam Pérez-Trujillo, Pau Nolis, Eva Monteagudo, Albert Virgili and Teodor Parella. ChemPhysChem,15 (2014) 854-857. DOI: 10.1002/cphc.201301130 A frequency-selective 1D 1H NMR experiment for the fast and sensitive determination of chemical shift differences between overlapped resonances is proposed. The resulting fully homodecoupled 1H resonances appear as resolved … Continue reading Rapid and efficient enantiodifferentiation through frequency-selective pure-shift ¹H NMR spectroscopy →

Easy measurement of one-bond proton-carbon and geminal proton-proton coupling constants in diastereotopic methylene groups

2014-02-21Methods & Applications, Our Publications, Our ResearchE.COSY, inverse INEPT, methylene spin systems, one-bond proton-carbon coupling constants, residual dipolar couplings, two-bonds proton-proton coupling constantsJosep

“Straightforward measurement of individual 1J(CH) and 2J(HH) in diastereotopic CH2 groups” by Josep Saurí, Laura Castañar, Pau Nolis, Albert Virgili and Teodor Parella. Journal of Magnetic Resonance 242 (2014) 33–40. DOI: 10.1016/j.jmr.2014.02.003 The C-HA cross-peak corresponding to a diastereotopic CHAHB methylene spin system exhibits a characteristic 1:0:1 multiplet pattern along the indirect dimension of a ω1-coupled HSQC spectrum. Share this:Share

Pure Shift NMR & HOBS Experiments

2013-12-16Methods & Applications, Our Research, Seminarsband-selective, enhanced resolution, full sensitivity, HOBS, HOBS-HSQC, HOBS-TOCSY, homodecoupling, homonuclear decoupling, HSQC, multiple frequency pulses, proton-carbon coupling constants, pure-shift NMR, TOCSYLaura

SeRMN seminar Date: Monday 16th December, 2013 Hour: 10 am Location: SeRMN, Facultats de Ciències i Biociències, C2/-135 Speaker: Laura Castañar, SeRMN PhD Student & Teaching Assistant, Dept. of Chemistry. A NMR pulse scheme that provides full sensitivity in homodecouped band-selective NMR experiments is proposed. Share this:Share

Implementing homo- and heterodecoupling in region-selective HSQMBC experiments

2013-12-04Methods & Applications, Our Publications, Our Researchband-selective, HOBS, homonuclear decoupling, HSQMBC, IPAP, proton-carbon coupling constants, pure-shift NMR, resolution enhancement, sensitivity enhancementLaura

“Implementing homo- and heterodecoupling in region-selective HSQMBC experiments” by Laura Castañar, Josep Sauri, Pau Nolis, Albert Virgili and Teodor Parella. Journal of Magnetic Resonance 238 (2014) 63-69. DOI: 10.1016/j.jmr.2013.10.022 A NMR method to enhance the sensitivity and resolution in band-selective long-range heteronuclear correlation spectra is proposed. The excellent in-phase nature of the selHSQMBC experiment allows that homonuclear and/or … Continue reading Implementing homo- and heterodecoupling in region-selective HSQMBC experiments →

Full sensitivity and enhanced resolution in homodecoupled band-selective NMR experiments

2013-11-13Methods & Applications, Our Publications, Our Researchband-selective, enhanced resolution, full sensitivity, HOBS, HOBS-HSQC, HOBS-TOCSY, homodecoupling, homonuclear decoupling, HSQC, multiple frequency pulses, proton-carbon coupling constants, pure-shift NMR, sensitivity enhancement, TOCSYLaura

“Full sensitivity and enhanced resolution in homodecoupled band-selective NMR experiments” by Laura Castañar, Pau Nolis, Albert Virgili and Teodor Parella. Chem. Eur. J. 2013, 19, 17283-17286. DOI: 10.1002/chem.201303235 A NMR pulse scheme that provides full sensitivity in homodecouped band-selective NMR experiments is proposed. Share this:Share

Simultaneous multi-slice excitation in Spatially encoded NMR experiments

2013-10-14Methods & Applications, Our Publications, Our Researchmulti-slice selection, multiple frequency pulses, pure-shift NMR, spatial encodingTeo

“Simultaneous multi-slice excitation in Spatially encoded NMR experiments” by Laura Castañar, Pau Nolis, Albert Virgili and Teodor Parella. Chem. Eur. J. 2013, 19, 15472–1547. DOI: 10.1002/chem.201303272 A novel strategy to enhance the experimental sensitivity in spatially encoded NMR experiments has been developed. Share this:Share

Presentations at the SMASH NMR Conference 2013

2013-09-13News from the SeRMN, NMR Events & Courses, Our Researchmulti-slice selection, multiple frequency pulses, pure-shift NMR, selective-excitation, spatial encoded nmrLaura

Next week several SeRMN members will present our research work at the SMASH NMR Conference 2013 that will take place in Santiago de Compostela (Spain) from 22nd to 25th September. Find below a summary of our contributions. Share this:Share

Simultaneous multi-slice excitation in spatially encoded NMR experiments

2013-08-29Our Research, SeminarsHSQMBC, multi-slice selection, multiple frequency pulses, pure-shift NMR, spatial encodingLaura

SeRMN seminar Date: Thursday 5th September, 2013 Hour: 10 am Location: SeRMN, Facultats de Ciències i Biociències, C2/-135 Speaker: Laura Castañar, SeRMN PhD Student & Teaching Assistant, Dept. of Chemistry. Share this:Share

Presentations to the EUROMAR 2013 Conference

2013-06-20News from the SeRMN, NMR Events & Courses, Our ResearchLaura

In a few days several SeRMN members will present our research work at the annual meeting of the European magnetic resonance community EUROMAR 2013 Conference that will take place in Hersonissos, Crete (Greece) from 30th June to 5th July. Find below a summary of our contributions. Share this:Share

Ultrafast 2D NMR

2013-04-25SeminarsLaura

SeRMN seminar Date: Friday 26th April, 2013 Hour: 10 am Location: SeRMN, Facultats de Ciències i Biociències, C2/-135 Speaker: Laura Castañar, SeRMN PhD Student & Teaching Assistant, Dept. of Chemistry. Share this:Share

SeRMN – NMR Service at UAB

Research & development, training, and facility management

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