In the following links one can find Data Set Examples of each Publication presented in the Thesis Work, as well as the corresponding Pulse Program Code for Bruker. All spectra have been previously phased and 2ii, 2ir, and 2ri files removed, otherwise data sets would be too big.
Publication 1: CLIP-HSQMBC: Easy measurement of small proton-carbon coupling constants in organic molecules. J. Saurí, T. Parella, J. F. Espinosa. Org. Biomol. Chem. 2013, 11, 4473-4478. DOI: 10.1039/C3OB40675J
Publication 2: A definitive NMR solution for a simple and accurate measurement of the magnitude and the sign of small heteronuclear coupling constants on protonated and non-protonated carbons. J. Saurí, J. F. Espinosa, T. Parella. Angew. Chem. Int. Ed., 2012, 51, 3919 –3922. DOI: 10.1002/anie.201108959
Publication 3: Efficient measurement of the sign and the magnitude of long-range proton-carbon coupling constants from a spin-state-selective HSQMBC-COSY experiment. J. Saurí, T. Parella. Magn. Reson. Chem. 2012, 50, 717–721. DOI: 10.1002/mrc.3867
Publication 4: Efficient and fast sign-sensitive determination of heteronuclear coupling constants. J. Saurí, P. Nolis, T. Parella. J. Magn. Reson. 2013, 236, 66–69. DOI: 10.1016/j.jmr.2013.08.013
Publication 5: On the interference of J(HH) modulation in HSQMBC-IPAP and HMBC-IPAP experiments. J. Saurí, T. Parella. Magn. Reson. Chem. 2013, 51, 509–516. DOI: 10.1002/mrc.3977
Publication 6: P.E.HSQMBC: Simultaneous measurement of proton-proton and proton-carbon coupling constants. J. Saurí, P. Nolis, L. Castañar, A. Virgili, T. Parella. J. Magn. Reson. 2012, 224, 101–106. DOI: 10.1016/j.jmr.2012.09.007
Publication 7: Simultaneous measurement of J(HH) and two different nJ(CH) coupling constants from a single multiply-edited 2D cross-peak. J. Saurí, T. Parella. Magn. Reson. Chem. 2013, 51, 397–402. DOI: 10.1002/mrc.3960
Publication 8: Straightforward measurement of individual 1J(CH) and 2J(HH) in diastereotopic CH2 groups. J. Saurí, L. Castañar, P. Nolis, A. Virgili, T. Parella. J. Magn. Reson. 2014, 242, 33–40. DOI: 10.1016/j.jmr.2014.02.003
On the other hand, this link contains a png file with 1H NMR and 13C NMR assignments for Strychnine and 2-Fluoropyridine compounds.
© 2014 – 2016, Josep. All rights reserved by the author(s) and Universitat Autonoma de Barcelona except for texts and images already copyrighted by third parties (e.g. journal publishers) and used here under the fair use provision.