PhD Thesis by Josep Saurí: Pulse Programs and Data Set Examples

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In the following links one can find Data Set Examples of each Publication presented in the Thesis Work, as well as the corresponding Pulse Program Code for Bruker. All spectra have been previously phased and 2ii, 2ir, and 2ri files removed, otherwise data sets would be too big.

Publication 1CLIP-HSQMBC: Easy measurement of small proton-carbon coupling constants in organic molecules. J. Saurí, T. Parella, J. F. Espinosa. Org. Biomol. Chem. 2013, 11, 4473-4478. DOI: 10.1039/C3OB40675J

Publication 2: A definitive NMR solution for a simple and accurate measurement of the magnitude and the sign of small heteronuclear coupling constants on protonated and non-protonated carbons. J. Saurí, J. F. Espinosa, T. Parella. Angew. Chem. Int. Ed., 2012, 51, 3919 –3922. DOI: 10.1002/anie.201108959

Publication 3Efficient measurement of the sign and the magnitude of long-range proton-carbon coupling constants from a spin-state-selective HSQMBC-COSY experiment. J. Saurí, T. Parella. Magn. Reson. Chem. 2012, 50, 717–721. DOI: 10.1002/mrc.3867

Publication 4Efficient and fast sign-sensitive determination of heteronuclear coupling constants. J. Saurí, P. Nolis, T. Parella. J. Magn. Reson. 2013, 236, 66–69. DOI: 10.1016/j.jmr.2013.08.013

Publication 5On the interference of J(HH) modulation in HSQMBC-IPAP and HMBC-IPAP experiments. J. Saurí, T. Parella. Magn. Reson. Chem. 2013, 51, 509–516. DOI: 10.1002/mrc.3977

Publication 6P.E.HSQMBC: Simultaneous measurement of proton-proton and proton-carbon coupling constants. J. Saurí, P. Nolis, L. Castañar, A. Virgili, T. Parella. J. Magn. Reson. 2012, 224, 101–106. DOI: 10.1016/j.jmr.2012.09.007

Publication 7Simultaneous measurement of J(HH) and two different nJ(CH) coupling constants from a single multiply-edited 2D cross-peak. J. Saurí, T. Parella. Magn. Reson. Chem. 2013, 51, 397–402. DOI: 10.1002/mrc.3960

Publication 8Straightforward measurement of individual 1J(CH) and 2J(HH) in diastereotopic CH2 groups. J. Saurí, L. Castañar, P. Nolis, A. Virgili, T. Parella. J. Magn. Reson. 2014, 242, 33–40. DOI: 10.1016/j.jmr.2014.02.003

On the other hand, this link contains a png file with 1H NMR and 13C NMR assignments for Strychnine and 2-Fluoropyridine compounds.